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Representative results require adequate sample preparation

The following situation is typical for many production plants: After a routine quality check, the production process is stopped or an already produced batch is suspended, because the analysis results were not within the relevant critical values. But does the tested product really deviate from the specifications? It is often not the product itself which causes irregular analysis results but a lack of understanding of the steps which come before the analysis.

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ホワイトペーパー (3)

  • White Paper. Different sieving methods for a variety of applications

    The determination and knowledge of the particle size distribution is an essential part of the quality control process for industrial products. Easy handling, low investment cost and high accuracy make sieve analysis one of the most frequently used procedures for measuring the particle size. This white paper gives an overview of the different sieving techniques and describes the necessary steps to ensure reliable results.
  • White Paper: Cryogenic Preparation of Sample Materials

    A solid sample material should always be sufficiently prepared by size reduction and homogenization before it is subjected to chemical or physical analysis. Care should be taken that the analysis sample fully represents the original material and that the sample preparation process is carried out reproducibly. Most sample materials can be reduced to the required analytical fineness at room temperature by choosing a mill with a suitable size reduction principle (impact, pressure, friction, shearing, cutting).
  • 食品分析 再現性の高い試料 信頼性の高い 分析のための準備

    Food occurs in a great variety of consistencies and is often inhomogeneous. Food testing labs require representative samples to produce meaningful and reproducible analysis results. Therefore, food samples must be homogenized and pulverized to the required analytical fineness, ideally with as little time and effort as possible.

パンフレット (2)

情報誌 "the sample" (1)

  • No. 43

    レッチェ粉砕機を使った、 代表性の高い食品分析の前処理
    [詳細...]

アプリケーションレポート (20)

  • エアジェットシーブAS200ジェットを使った凝集粉末の分級

    エアジェットシーブは、40μm以下の非常に細かい粉体の乾式分級に広く用いられています。また、振動式のふるい振とう機に比べて極めて短時間で分級ができるので、250μmまでの粉体にも広く採用されています。
  • カカオ畑から板チョコへ

    カカオの実からチョコレートになるまでは、長 い工程を経ます。収穫、醗酵、乾燥、洗浄、焙 煎、摩砕、そしてさらにそのカカオ片を粉砕し て、カカオ粉とカカオバターからなる濃縮液と なり、最終的にプレス成形されます。その間、 それぞれの工程で品質が管理されています。製 品に有害物質(カビや重金属)が含まれていな いか、また、成分(油脂や炭水化物)を検査す るだけでなく、ココアの滑らかさを見るために 適切な粒度にまで細かく粉砕されているかどう かまで検査します。人間の味覚は30μm以下 の小さい粒子を好むので、粒度もまた重要な要 素なのです。
  • カッティングミルSM300伝統からの革新

    カッティングミルは試料調製に広く使われている粉砕機です。二次燃料の粉砕、再生可能な
    バイオマスの研究開発、WEEE/RoHS対応の成分分析および有価金属の回収など、その
    アプリケーションは多岐にわたります。
  • クライオミルを使った揮発性物質を含んだ試料の粉砕

    試料調製の際に、常温での粉砕よりも凍結粉砕機を使ったほうが適している場合がありま
    す。液体窒素で凍結された試料は脆化されるので、衝撃・摩擦などで粉砕されやすくなり
    ます。さらに、試料中の揮発性物質も保持できます。
    レッチェのクライオミルは、最新の安全な凍結粉砕機で優れた粉砕結果をお約束します。
  • シリアルバーの成分分析

    シリアルバー等の食品は、しばしば「低カロリー」や「健康」を謳われます。本当に「低カロリー」
    で「健康」であるかを確かめるためには、食品の品質管理で重要な科学的な分析が必要です。パッ
    ケージには、100gや100mLあたりの脂質、脂肪酸、糖質、および塩分等の平均含有量が表示して
    あります。シリアルバーには、色々な物(ナッツ、レーズン、オートフレーク等)が混在している
    ので、正確な分析結果を得るためには、完璧な分析試料のホモジナイジングが必要になります。
  • 食品の完全なホモジナイズの為に

    Die neue Messermühle GRINDOMIX GM 200 homogenisiert selbst schwierigste Proben vollständig und sorgt so für Analysenergebnisse mit minimaler Standardabweichung. Der Bericht zeigt anhand von Applikationsbeispielen, z. B. Speck und Rosinen, wie sich dank neuer Leistungsmerkmale homogene Proben in maximal zwei Arbeitsschritten herstellen lassen.
  • 食品・飼料の肥質分析

    食品や飼料の品質を管理するうえで、脂質は非常に重要な分析項目です。脂肪量は薬品の栄養価を大きく左右する要素であり、また、乳脂肪やカカオバターなどの比較的高価な脂肪分は、効率よく利用する必要があります。加えて、新しいEU指令によって食品会社は「ライト」や「低脂肪」などの抽象的は表示ではなく、正確な脂肪分を包装に表示するように求められています。
  • Air Jet Sieving of Bulk Materials

    Particle size analysis and particle size distribution are important criteria for the quality control of bulk materials. In a running production process, the results of a quality check must be available quickly to allow for immediate adjustment of the production parameters. Depending on the expected particle size and sample volume, different sieving methods and sieving machines are suitable for analysis. The method used for particle size analysis is primarily determined by the fineness of the material to be sieved. For dry sieving of samples with particle sizes below 40 microns, air jet sieving is the method of choice.
  • Contamination-free cutting of raw materials for the food and medical industries with the new SM 300 foodGrade

    Raw materials for the food or pharma industry often require a size reduction process to minimize the particle size (tea, herbs, spices). The materials can be ready for consumption, like tea, or they are used for a second processing step, like extraction of valuable ingredients. A current example is CBD oil extraction from ground cannabis plants. For both – direct use or process step prior to extraction, the specific requirements of the food and medical industries must be considered when choosing a suitable size reduction tool. Aspects like smooth surfaces, easy cleaning, and available materials like stainless steel 316L to ensure contamination-free processing should be taken into account. Retsch has launched the new Cutting Mill SM 300 foodGrade for this type of applications and small-scale production of herbs and spices.
  • Food samples - safe and efficient cryogenic grinding

    Most sample materials can be ground to the required analytical fineness at room temperature. However, there are limits, for example when even a small temperature increase affects the sample in a negative way; or when the material is very elastic and will only be deformed. Moreover, food samples which are fatty or sticky may block the mill. Therefore, cryogenic grinding is the best way to pulverize food samples like cheese, raisins, wine gum or marzipan which simply clump together when ground at room temperature.
  • Genetically modified organisms (GMO) - detection in food and feed samples

    Genetic engineering opens up new possibilities in areas such as medical research, development of alternative fuels or global food supply. It is used to modify the characteristics of plants in order to increase the crop yield, improve defense against predators, pesticides or draught, but also increase concentrations of essential vitamins. However, with regards to food the use of genetic engineering is a fairly controversial issue.
  • Measuring Dust - Incoming Inspection with Sieve Analysis

    Graduate student Jennifer Franz has developed a new inspection procedure during her work at the German food producer Lebensgarten GmbH. With the help of sieve analysis the company can now reliably ascertain the fines and dust fractions of incoming cereal flakes; these have a negative influence on the mixing and packaging process of muesli.
  • Mixer Mill MM 400: Upgrade of a True Multipurpose Mill

    With the Mixer Mill MM 400 RETSCH has developed a true multipurpose mill which covers a huge range of applications, including classic mixing and homogenization but also more complex tasks like cell disruption via bead beating or mechanochemical processes. The ease of use of mixer mills in general, combined with a wealth of accessories make the MM 400 the perfect choice for quick, safe and reproducible processing of small sample volumes.
  • Particle size - a quality feature

    The determination of the particle size distribution of a product has always been of great significance in food production. Taste, color, solubility or extraction behavior are only a few examples of product properties which are directly influenced by particle size. In the testing laboratory of the St. Petersburg branch of LLC Wrigley, RETSCH sieve shakers AS 200 jet and AS 200 control are utilized for particle size analysis of fine powders which are used for chewing gum production.
  • Quick and reproducible grinding of feedstuff

    Grain, compound feeds or feed pellets occur in a variety of forms; compound feeds are usually inhomogeneous. Feedstuff is analyzed, for example, to determine the nutritional value, to detect hazardous substances or genetically modified ingredients. To ensure meaningful and reliable analysis results, representative and homogeneous samples are required. Therefore, sample preparation involves homogenization and size reduction of the material to a defined particle size. RETSCH laboratory mills are perfectly suited for this process.
  • Representative results require adequate sample preparation

    The following situation is typical for many production plants: After a routine quality check, the production process is stopped or an already produced batch is suspended, because the analysis results were not within the relevant critical values. But does the tested product really deviate from the specifications? It is often not the product itself which causes irregular analysis results but a lack of understanding of the steps which come before the analysis.
  • Reproducible and convenient sample preparation for reliable food analysis

    Reliable analytical results can only be guaranteed if the entire sample preparation process is reproducible. A well-known standard in sample preparation of foodstuffs are ultra-centrifugal mills, which are used for rapid pulverization of soft, medium-hard, brittle and fibrous food. Retsch’s latest model, the ZM 300, offers decisive advantages for food analysis such as temperature monitoring for temperature-sensitive materials, improved sample throughput and well-thought-out handling for particularly ergonomic working.
  • Reproducible and reliable sample preparation

    In the book "Ideas and Applications Toward Sample Preparation for Food and Beverage Analysis," (ISBN 978-953-51-3686-6), edited by Mark T. Stauffer, RETSCH has published a chapter on reliable sample preparation of food samples. This chapter describes the process of turning a laboratory sample into a representative part sample with homogeneous analytical fineness by choosing the most suitable mill. Important aspects of size reduction and homogenization are explained, a variety of application examples is given, and specific applications such as cryogenic grinding are discussed in detail.
  • Sample Division of Large Volumes

    Representative sampling of large sample volumes is an integral part of the physical and chemical analysis of bulk goods and has a decisive influence on the quality of the results. Extraction of a sample from the bulk is not always carried out in a way to ensure representativeness. This is a widespread flaw in the quality control process with a negative impact on the subsequent analysis results. RETSCH provides some convenient solutions which help to improve working conditions and thereby the quality of the sampling process.
  • Sticky, tough, moist – cryogenic homogenization of food samples

    The homogenization of food samples is a crucial step prior to the actual analysis. Due to the various properties of food – dry, moist, sticky, tough, hard, soft, etc. – a versatile laboratory mill is required to ensure reproducible preparation of the analytical sample. RETSCH’s knife mill GRINDOMIX GM 200 is employed in laboratories all over the world for the homogenization of food samples as well as samples with a high water, oil, sugar or fat content. This mill covers a wide application range, from granular products like rape seed, rice, soybeans to fibrous or tough samples like meat, fish, candy, cheese or plants.

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