試料分析方法XRFに関する情報

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  • White Paper: How to minimize standard deviations by correct sample preparation

    Modern analytical methods increase precision and push detection limits to make even the smallest traces of sample components detectable. Despite this development sample preparation, which is carried out prior to the actual analysis, is frequently neglected. Errors caused by lacking accuracy in sample preparation have a much bigger impact than errors made during analysis. Just like an iceberg which is mostly hidden under water, only a small part of the sum of errors is perceived whereas the major part of potential errors is not taken into account (fig. 1). One of the reasons may be the fact that sampling and sample preparation have always been done in a traditional way which has become a routine over the years and is no longer considered as having a critical influence on the subsequent analyses.

アプリケーションレポート (4)

  • できる限り純粋に

    理想的な状態で粉砕が行われても、試料と粉 砕容器の表面がこすれて起きる機械的ストレ スによって粉砕容器の表面が摩耗します。し かし、粉砕機と粉砕容器を適切に選択するこ とで、この摩耗を軽減することは可能です。 もし試料を100μm未満に粉砕する必要があ る場合は、非常に強い力が必要なので、その 分、摩耗も大きくなります。
  • 蛍光X線分析用の試料調製

    蛍光X線分析は質量分析に広く使われている分析方法ですが、試料調製が正しく行われないと正確で再現性の高い分析結果が得られません。
  • The effect of grinding tools on metal contamination

    Reliable and accurate analysis results can only be guaranteed by reproducible sample preparation. This consists of transforming a laboratory sample into a representative part sample with homogeneous analytical fineness. Retsch offers a comprehensive range of the most modern mills and crushers for coarse, fine and ultra-fine size reduction of almost any material. The product range also comprises a wide choice of grinding tools and accessories which helps to ensure contamination-free preparation of a great variety of sample materials.
    The selection of the correct grinding tool depends on the sample material and the subsequent method of analysis. Different grinding tools have different characteristics, such as required energy input, hardness or wear-resistance.
  • Representative sample preparation for XRF analysis

    Preparing homogeneous samples by milling

使用事例 (2)